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important to note that the occupancy of Ba2+ in every site is the same, and the value is about 0.56, indicating that the established structure is suitable. With respect to the Rietveld method, the powder patterns were analysed using the materials studio program running on a personal computer. The Rietveld refinement details for BaGdF5 are presented in Table 1. The final fitting factors are Rp=4.97%, Rwp=6.62%, et al., and indicate the disordered structure of BaGdF5 is conceivable.22 |
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